All the reagents were used without further purification unless otherwise specified. All aqueous solutions were prepared with twice-distilled water throughout the whole experiments. Preparation of ethaline ChCl was recrystallized from absolute ethanol, and then filtered and dried under a vacuum. EG was dried under a vacuum prior to use.
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John Wiley [distributor], Public Private login e. SearchWorks Catalog To include a comma in your tag, surround the tag with double quotes. These online bookshops told us they have this item: Electroreduction of Sulfur, Selenium, and Tellurium Compounds.
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Tags What are tags? Electroreduction of Synthfsis Compounds. Electroreduction of Nitrogen Compounds. Electroreductive Reaction of Olefins. Describe the connection issue. Login to add to list. Separate different tags with a comma. In order to set up a list of libraries that you have access to, you must first login or sign up. SearchWorks Catalog Stanford Libraries. Besides a plethora of modern reaction methods, it also treats such other important aspects as product selectivity, types of electrolysis cells and effects of additives.
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Electroorganic reduction synthesis
Experimental setup[ edit ] The basic setup in electrosynthesis is a galvanic cell , a potentiostat and two electrodes. Typical solvent and electrolyte combinations minimizes electrical resistance. Aprotic conditions often use an organic solvent such as acetonitrile or dichloromethane with electrolytes such as lithium perchlorate or tetrabutylammonium salts. The choice of electrodes with respect to their composition and surface area can be decisive. For example, in aqueous conditions the competing reactions in the cell are the formation of oxygen at the anode and hydrogen at the cathode. In this case a graphite anode and lead cathode could be used effectively because of their high overpotentials for oxygen and hydrogen formation respectively.
In order to set up a list of libraries that you have access to, you must first login or sign up. John Wiley [distributor], c Electroreduction of Nitrogen Compounds. Comments and electroodganic What are comments? Electroreductive Reaction of Aromatic Compounds. With its clear structure and its focus on synthetic methods, this is a source of high quality information for every chemist working in this field. Besides a plethora of modern reaction methods, it also treats such other important aspects as product selectivity, types of electrolysis cells and effects of additives. SearchWorks Catalog Stanford Libraries.